Measuring flask, 1000 ml, made of laboratory glass, with plastic stopper
This unused piston is made of heat-resistant laboratory glass and comes from stocks of the former GDR. It is particularly suitable for the collection of hydrolates in the distillation. It has exactly the size of the maximum removal quantity of the message-free 2-liter stills.
Product No.:
450.211
Shippingtime:
2 - 4 working days, available from stock
Accessory set with pump for miniature copper stills up to 3 litres- Not suitable for our stainless steel stills This set includes everything you need to be able to distil immediately and seriously with our stills up to about 3 litres. The pump is powerful enough to safely supply even all mini nestling in the range 0,5 to 3 litres size (as they may be used legally in Austria and from 2018 Germany or Switzerland) with cooling water. First and foremost, the set contains a functionally-sized cooling system for the still, but there are also other accessories for cleaning and sealing. In addition, when purchasing a stainless steel still together with the accessory set the right hose fittings for our coolers are there.
The set includes a 10-liter plastic tub as a cooling water depot (the water must be replaced several times in larger distilleries), plus a 230-volt cooling water pump, plus several meters of food-grade tubing in four different sizes so you can safely connect any distillery. The hoses can be partially inserted into each other and can thus also bridge different connections and adapters. In addition, a cleaning brush, a swim thermometer, a roll of Teflon tape for sealing the still and a 100 ml graduated cylinder to the distillate safely collecting and measuring.
Product No.:
109.301
Shippingtime:
2 - 4 working days, available from stock
Cooling set with pump for our stainless steel distillers up to 20 litres
This set contains everything you need to start serious distillation immediately, even with our unobtrusive 2-litre stainless steel distillers.
Set accessories
20 litre plastic tub as cooling water reservoir
Powerful 230V cooling water pump with accessories for different hose diameters, sufficient for all our stainless steel stills up to 10 litres.
Various 2m PVC hoses, 2 of which have hose fittings for the still cooler:
The first hose goes from the pump to the 1/2‘ connection of the condenser near the distillate outlet at the bottom. The second hose is connected to the 1/2’ connection for the hot waste water at the top of the condenser. The other end with the 3/4‘ connection is led to where the waste water should go, so back into the bucket when pumping. The 3/4’ connection is now new - previously this end remained open. The reason for this innovation is that you can replace the hoses if you have running water nearby. Most house connections have a 3/4’ thread, so you can connect the 2nd hose from the running water supply to the water inlet of the cooler. The 1st hose is then connected to the top of the cooler and the hot waste water now comes out of the black pump screw nipple. The pump is not needed for this cooling variant. So you now have two options for cooling. In addition to these two hoses, there are three hoses of different strengths for various applications.
Plastic tap for cooling water control, suitable for the counterflow cooler.
Scaled 100 ml measuring cylinder with foot to safely collect and measure the distillate.
Cleaning brush.
Floating thermometer for cooling water control if the hot waste water is allowed to flow back into the bucket. From 40° C, the water should either be cooled with ice or replaced.
A roll of Teflon tape for sealing, e.g. if a seal fails during distillation.
Product No.:
109.301.2
Shippingtime:
2 - 4 working days, available from stock
Stainless steel burning protection The safest protection against burning of mash, when distilling, is a water bath still. But with directly heated boilers you must have devices that prevent burning with high security. The first step is to keep the thick components of a mash away from the heated bottom. This is achieved primarily by a mash strainer. But a mash strainer alone is not a 100% burning protection. If the liquid component of a mash still contains starch, the liquid can also burn. To find that out, you should either do an iodine starch test, or cheaper, put a small amount of the liquid mash in a small pot and do a burning test on the stove. If the small amount burns, precautions must be taken.
If you know that you do not use 100% ripe fruit, burn is likely. In this case, it is advisable to use an amylase, which converts residual starch into sugar. This not only reduces the danger of burning, but also increases the yield.
Nevertheless, you should perform the above-mentioned burning test after fermentation. If the sample still tended to burn despite using an amylase, in addition to the mash sieve for instance a mash bag, as we offer it here in different sizes. This can not only keep solid components off the ground, but also filter out residual yeast. The combination of amylase, mash screen and filter bag or filter cloth should prevent burning.
Aroma basket Is not it just protection against burning, but that either, in Germany only for commercial applications, alcohol vapor flows through fruits or herbs to obtain an aromatized distillate, or steam distillations to produce hydrosol and essential oils to be carried out, which is also in Germany is allowed, one uses a height-adjustable aroma sieve. This is placed in a still above the neutral alcohol or water and filled with fruits, flowers or herbs and will be distilled.
Lavender is a member of the mint family and is often used for perfume extraction.
You are purchasing a product that is ideally suited for the extraction of essential oils and fragrant hydrolates. The aroma-protected and light-protected packaging ensures a consistently excellent quality for a long time.
Simply fill the flowers in the plant / drug room. The flowers must not be pressed. Close your system and distil at medium to high heat setting. For drug containers height> diameter, you can set the heating level higher. Find out the ideal distillation speed for your system yourself. The lavender flowers offered here have a high oil yield.
Product No.:
105.711
Shippingtime:
2 - 4 working days, available from stock
Oil separator / separating funnel 100 ml - according to Squibb
Oil separator made from DURAN BOROSILICATE GLASS 3.3 - laboratory quality. The optimal separating funnel for the clean separation of essential oil and hydrosol when distilling as well as other liquids with different weights (e.g. oil and water)
A separating funnel is an indispensable aid for the distillation of essential oils with many other uses in the laboratory and at home. This oil separator is resistant to most acids and heat-resistant even above 100 ° C.
Best quality so that you can enjoy your work for a long time.
DURAN BOROSILICATE GLASS 3.3
With PTFE laboratory stopcock (tap)
ground glass jointNS 29/32
Product No.:
105.701
Shippingtime:
9 to 14 working days, will be reordered or very long assembly time
Laboratory oil separator set for all hobby stills – for separating the oil after distillation A few tips before you start.
This set is suitable for easily separating the essential oil from the hydrosol after distillation. In addition to this set, it's best to have clean bottles ready for the final bottling. I use wine bottles with corks for the maturing period or flip-top bottles for final storage. No matter what, the main thing is that the bottles are light-protected. I simply cleaned the bottles with washing-up liquid and carefully rinsed them. In my experience, sterilising the bottles, as recommended in many sources, is not necessary. Light is the only enemy. If you plan to store the hydrosol in the Erlenmeyer flasks for several days, they should first be closed with stoppers rolled out of kitchen paper and stored in a dark place. After about a week, the hydrosol should be transferred to the coloured bottles for storage, or the paper stoppers should be dipped in stoppers 8.1 or 9.1. When storing in wine bottles, the cork can be used to seal the bottle. Over time, the cork will cause the hydrosol to mature, which will take no longer than three months. However, only hydrosols with a pH of ≤ 5 can be stored for longer periods. My oldest acidic hydrosols are now 4 years old and in very good condition. I stored them in the cellar at average temperatures below 18 °C. But even occasional temperatures of 22 °C did not harm these hydrolates. I also have hydrolates with 5.5 ≥ pH ≤ 6, which showed sensory signs of old varnish after one year, without completely turning over. However, you don't really want these hydrolates. In practice, the hydrolates are usually not stored for so long; for me, the goal was the long-term experiment.
Distillation
This set is very flexible and can be used for stills with a high distillate outlet and also when the outlet is low and a setup as shown above is not possible.
In the first case, use the Erlenmeyer flask as a receiver and collect 500 ml as the first batch. For stills with a high distillate outlet, you can also use the oil separator directly as a template, as shown above, and gradually drain the hydrolate into the Erlenmeyer flask. Depending on the still, the extraction takes 8 to 15 minutes. You can assume that the oil is included in this margin.
You can arrange to replace the Erlenmeyer flask for the second batch without interrupting the distillation. At the latest, you should hold a pH strip in the distillation jet in the middle of the second batch. You can use this value to decide whether a further batch is useful. If the pH value is below approx. 4.5, you can consider a further distillation run. For this, the distillation must be interrupted in the 2-litre hobby systems as a precaution in order to top up the water in the boiler. However, this is not a problem because no more oil can be lost. The distillation continues where you left off.
In my experience, in the vast majority of cases, the distillation was complete after removing two portions. I found one of the exceptions with fennel seeds.